华南理工大学学报(自然科学版) ›› 2021, Vol. 49 ›› Issue (3): 55-61.doi: 10.12141/j.issn.1000-565X.200241

所属专题: 2021年机械工程

• 机械工程 • 上一篇    下一篇

Nd: YAG 晶体表面性能等离子体改性研究

曹发祥 孔金星 杜东兴   

  1. 中国工程物理研究院 机械制造工艺研究所,四川 绵阳 621900
  • 收稿日期:2020-05-18 修回日期:2020-10-19 出版日期:2021-03-25 发布日期:2021-03-01
  • 通信作者: 孔金星(1976-),男,高级工程师,主要从事难加工材料的高速精密加工技术研究。 E-mail:kjxmc106@163.com
  • 作者简介:曹发祥(1997-),男,硕士生,主要从事硬脆材料磨削亚表面损伤控制方法研究
  • 基金资助:
    国家自然科学基金资助项目 ( 51805498) ; 中物院超精密加工技术重点实验室基金资助项目 ( K1154-1820- TCJ)

Research on Surface Properties of Nd: YAG Crystal Modified by Plasma Jet

CAO Faxiang KONG Jinxing DU Dongxing   

  1. Institute of Mechanical Manufacturing Technology,China Academy of Engineering Physics,Mianyang 621900,Sichuan,China
  • Received:2020-05-18 Revised:2020-10-19 Online:2021-03-25 Published:2021-03-01
  • Contact: 孔金星(1976-),男,高级工程师,主要从事难加工材料的高速精密加工技术研究。 E-mail:kjxmc106@163.com
  • About author:曹发祥(1997-),男,硕士生,主要从事硬脆材料磨削亚表面损伤控制方法研究
  • Supported by:
    Supported by the National Natural Science Foundation of China ( 51805498)

摘要: 采用自行研制的常温等离子设备,开展等离子体射流对 Nd: YAG 晶体表面润湿 性和表面力学性能的改性试验研究。结果表明: 等离子体对 Nd: YAG 晶体表面具有明 显的改性作用,等离子体改性后 3 种粗糙度特征的 Nd: YAG 表面润湿性均获得改善, 其中光滑表面由疏水转变为超亲水,且在 30 h 内保持良好的亲水状态,改性后 Nd: YAG 晶体表面含氧官能团的增加是润湿性改善的主要原因; Nd: YAG 晶体改性后 0 ~ 11 h、 11 ~ 22 h、22 ~ 35 h,显微硬度分别呈现出保持、下降与回复、稳定的特点,其中 11 ~ 22 h 内具有最低的表面显微硬度,在 15. 0、30. 0、70. 0 mN 载荷作用下,其平均显微硬 度分别下降了 56. 2% 、45. 0% 、31. 6% ; 改性后 11 h,表面塑性的迅速提高导致部分压 痕形貌出现 “阶梯”和 “阴影”特征。

关键词: 等离子体, 改性, Nd: YAG 晶体, 润湿性, 纳米压痕, 显微硬度

Abstract: The surface wettability and mechanical properties of Nd: YAG crystals were investigated to study the influence of plasma jet on Nd: YAG crystals by using self-developed plasma equipment at room temperature. The results show that the plasma has significant effects on surface properties of Nd: YAG crystals,and the wettability of Nd: YAG crystals with three different roughness is improved after plasma modification. Especially,the smooth surface changes from hydrophobic to super-hydrophilic,and the good state of hydrophilicity lasts 30 hours. The improvement of wettability of Nd: YAG surface mainly lies in the increase of oxygen-containing functional groups on the surface of the modified Nd: YAG crystals. The microhardness remains unchanged within 0 to 11h,decreases first and then increases within 11 to 22h,and remains stable within 22 to 35h after the modification. Especially,a minimal microhardness occurs between 11 to 22 h after the modification. Under the peak load of 15. 0,30. 0 and 70. 0mN,the average microhardness decreases by 56. 2%, 45. 0% and 31. 6%,respectively. And the morphology of some indentations shows features of“ladder”and“shadow” due to the rapid increase of plasticity on Nd: YAG surface 11 hours after the modification.

Key words: plasma, modification, Nd, YAG crystal, wettability, nanoindentation, microhardness

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