华南理工大学学报(自然科学版) ›› 2003, Vol. 31 ›› Issue (11): 92-96.

• • 上一篇    

TiO2 的微波辐射 So-l Gel 法制备及其光催化性能

夏启斌 李 忠 奚红霞 徐科峰 肖 静   

  1. 华南理工大学 化工学院‚广东 广州510640
  • 出版日期:2003-11-20 发布日期:2022-06-17
  • 作者简介:夏启斌(1974-)‚男‚博士生‚主要从事环境工程和化学工程研究.

Preparation and Photocatalysis Characterization of TiO2by Microwave Radiation So-l Gel Method

Xia Q-i bin Li Zhong Xi Hong-xia X u Ke-feng Xiao Jing   

  1. College of Chemical Engineering‚South China University of Technology‚Guangzhou510640‚China
  • Online:2003-11-20 Published:2022-06-17

摘要: 采用微波辐射 So-l Gel 法在石英砂表面制备负载型 TiO2 光催化剂‚考察不同加 热方式‚微波功率以及微波加热温度对溶胶质量的影响‚微波加热反应制备的溶胶粒子平 均粒径小于常规加热反应制备得到的溶胶粒子‚微波加热反应适宜条件是微波功率 600W‚反应温度为90℃.以苯酚为光催化降解研究对象‚考察了两种方式制备的负载型 TiO2 光催化剂的催化性能‚实验结果表明微波辐射 So-l Gol 法制备的负载型 TiO2 光催 化剂光催化性能也优于常规 So-l Gel 法制备的负载型 TiO2 光催化剂.

关键词: 二氧化钛, 微波, So-l Gel 法, 光催化

Abstract: Titanium dioxide(TiO2) photocatalysts have been deposited on quartz sands by microwave radiation So-l Gel method.The influencing factors on sol quality including different heating-up method‚ microwave power and microwave reaction temperature have been investigated.The particle size in the sol prepared by microwave radiation is smaller than the one by normal heating-up method.The appropriate microwave reaction conditions are the microwave power of 600W and90℃.Phenol is regarded as the photodegradation reactant and the photocatalysed performances of two photocatalysts prepared by two different methods have been investigated .The results indicate that the photocatalysed performance of TiO2 photocatalysts prepared by microwave radiation So-l Gel method is better than the one prepared by conventional So-l Gel method.

Key words: titanium dioxide, microwave, So-l Gel method, photocatalysis

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