华南理工大学学报(自然科学版) ›› 2014, Vol. 42 ›› Issue (5): 41-47.doi: 10.3969/j.issn.1000-565X.2014.05.007

• 环境科学与技术 • 上一篇    下一篇

废弃烟梗和烟末中主要化学组分的浸渍提取

高文花1,2 陈克复1 叶代启2 杨仁党1 杨飞1   

  1. 1.华南理工大学 制浆造纸工程国家重点实验室,广东 广州 510640;2.华南理工大学 环境与能源学院,广东 广州 510006
  • 收稿日期:2013-10-15 修回日期:2014-03-09 出版日期:2014-05-25 发布日期:2014-04-01
  • 通信作者: 高文花(1987-),女,博士后,主要从事植物资源综合利用研究. E-mail:gaowenhua2010@gmail.com
  • 作者简介:高文花(1987-),女,博士后,主要从事植物资源综合利用研究.
  • 基金资助:

    “十二五” 国家科技支撑计划重点项目(2013BAC01B03);华南理工大学中央高校基本科研业务费专项资金资助项目(2014ZB008, 2014ZZ0062)

Macerated Extraction of Main Chemical Components from Abandoned Tobacco Stems and Leave Powders

Gao Wen- hua1,2 Chen Ke- fu1 Ye Dai- qi2 Yang Ren- dang1 Yang Fei1   

  1. 1.State Key Laboratory of Pulp and Paper Engineering,South China University of Technology,Guangzhou 510640,Guangdong,China; 2.College of Environment and Energy,South China University of Technology,Guangzhou 510006,Guangdong,China
  • Received:2013-10-15 Revised:2014-03-09 Online:2014-05-25 Published:2014-04-01
  • Contact: 高文花(1987-),女,博士后,主要从事植物资源综合利用研究. E-mail:gaowenhua2010@gmail.com
  • About author:高文花(1987-),女,博士后,主要从事植物资源综合利用研究.
  • Supported by:

    “十二五” 国家科技支撑计划重点项目(2013BAC01B03);华南理工大学中央高校基本科研业务费专项资金资助项目(2014ZB008, 2014ZZ0062)

摘要: 浸渍提取是制备造纸法烟草薄片的重要环节,浸渍提取液是高质量薄片涂料的主要组分来源.文中结合生产实际,以水作为提取剂,采用正交实验和单因素实验相结合的方法,研究了不同的浸渍温度、浸渍时间和浸渍液比条件下废弃烟梗和烟末中主要化学组分的溶出规律,得到了烟梗和烟末一段浸渍提取的最优条件:烟梗浸渍时间为100min,浸渍温度为 60℃,浸渍液比为 1∶ 7,此时水溶性糖和总植物碱的溶出率分别达到 50.60%和 52.46%;烟末浸渍时间为60min,浸渍温度为70℃,浸渍液比为1∶ 10,此时水溶性糖和总植物碱的溶出率分别达到 73.06%和 64.57%.

关键词: 烟草薄片, 烟梗, 烟末, 浸渍提取, 组分, 溶出率

Abstract:

Macerated extraction is an important step of producing reconstituted tobacco sheets by paper- makingtechnology,and the extracting solution is also a major ingredient for making high- quality reconstituted tobacco coa-tings.In this paper,the main chemical components in abandoned tobacco stems and leave powders were extractedby combining an orthogonal test with single- factor experiments,with water as the solvent.Then,the effects ofmaceration time,maceration temperature and solid/liquid ratio on extraction rate were investigated,and the optimalmacerated extraction conditions for abandoned tobacco stems and leave powder were determined.The results showthat,under the optimal conditions for abandoned tobacco stems,i.e.,a maceration time of 100 min,a macerationtemperature of 60℃ and a solid/liquid ratio of 1∶ 7,the dissolution rates of water- soluble sugars and total alkaloidare 50.60% and 52.46%,respectively; and that the dissolution rates respectively reaches 73.06% and 64.57%under the optimal conditions for abandoned tobacco leave powders,that is,a maceration time of 60 min,a macera-tion temperature of 70℃ and a solid/liquid ratio of 1∶ 10.

Key words: reconstituted tobacco sheet, tobacco stem, tobacco leave powder, macerated extraction, components, dissolution rate

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