华南理工大学学报(自然科学版) ›› 2009, Vol. 37 ›› Issue (4): 120-124.

• 食品科学与技术 • 上一篇    下一篇

冷冻环境对湿面筋蛋白中可冻结水的影响

宋国胜1,2  胡松青1  李琳1  郭祀远1   

  1. 1. 华南理工大学 轻化工研究所, 广东 广州 510640; 2. 华南理工大学 分析测试中心, 广东 广州 510640
  • 收稿日期:2008-04-02 修回日期:2008-06-30 出版日期:2009-04-25 发布日期:2009-04-25
  • 通信作者: 胡松青(1972-),男,博士,副教授,主要从事分离与纯化的理论与技术、功率超声在生物化工和食品化工中的应用等研究.E-mail:fesqhu@scut.edu.cn E-mail:gssong@scut.edu.cn
  • 作者简介:宋国胜(1966-),男,博士生,工程师,主要从事分离原理与技术研究.
  • 基金资助:

    国家自然科学基金资助项目(20436020,20506006)

Effects of Freezing Conditions on Freezable Water in Wet Gluten

Song Guo-sheng 1.2 Hu Song-qing1  Li Lin1  Guo Si-yuan1    

  1. 1. Research Institute of Light Industry and Chemical Engineering, South China University of Technology, Guangzhou 510640, Guangdong, China ; 2. Analytical and Testing Center, South China University of Technology, Guangzhou 510640, Guangdong, China
  • Received:2008-04-02 Revised:2008-06-30 Online:2009-04-25 Published:2009-04-25
  • Contact: 胡松青(1972-),男,博士,副教授,主要从事分离与纯化的理论与技术、功率超声在生物化工和食品化工中的应用等研究.E-mail:fesqhu@scut.edu.cn E-mail:gssong@scut.edu.cn
  • About author:宋国胜(1966-),男,博士生,工程师,主要从事分离原理与技术研究.
  • Supported by:

    国家自然科学基金资助项目(20436020,20506006)

摘要: 用差示扫描量热仪测定了不同冷冻环境下湿面筋蛋白中可冻结水的含量,探讨了超声辅助食品冷冻过程中冰结晶的热力学机制;用扫描电镜间接观察和分析了冷冻湿面筋蛋白中冰晶的形状和粒度分布.结果表明:360W、440W超声辅助冷冻和液氮浸渍冷冻的湿面筋蛋白中可冻结水占总水含量的比例分别为67.3%、70.8%和77.0%,均比传统冷冻过程的(56.9%)高;不同环境下冷冻的样品其热力学特征各不不同;适宜功率的超声能加速湿面筋蛋白的冷冻过程,削弱面筋蛋白和水分子之间的相互作用力;超声辅助和液氮浸渍冷冻的湿面筋蛋白中冰晶细小,直径在4μm以内且分布均匀,可减少对面筋蛋白网络结构的破坏;与高能耗的液氮浸渍冷冻法相比,超声辅助冷冻是一种更实用的改善食品品质的技术.

关键词: 湿面筋蛋白, 超声, 冷冻, 冰晶, 可冻结水

Abstract:

The content of freezable water in frozen wet gluten was determined by means of differential scanning calorimetry (DSC) to reveal the thermodynamic mechanism of ice crystallization during the ultrasonic-assisted food freezing. The shape and size distribution of ice crystals in the frozen wet gluten were also studied by means of scan- ning electron microscopy. It is found that  the freezable water contents (relative to the total water content) of wet gluten frozen respectively with an ultrasonic-assisted process respectively at 360 W, 440 W and a liquid nitrogen freezing process, namely 67.3% , 70.8% and 77.0% , are higher than that with the traditional freezing process (56. 9% ) ;  the samples frozen in different conditions are of different thermodynamic characteristics;  ultrasonic with suitable power accelerates the freezing of wet gluten and weakens the interaction between gluten and water molecules;  both the ultrasound-assisted and the liquid nitrogen freezing processes result in well-distributed ice crystals with a small size less than 4 μm, thus reducing the deterioration of gluten network ; and  as compared with the liquid nitrogen freezing process with high energy consumption, the ultrasound-assisted freezing process is more practical for food quality improvement.

Key words: wet gluten, ultrasonic, freezing, ice crystal, freezable water