利用高压反应釜在氢气气氛 2MPa、温度 260℃、时间 80min、转速 450r/min 的条 件下，对 1-烯丙基-3-甲基咪唑醋酸盐(［AMIM］OAc)预处理竹粉后的再生木质素进行氢 解． 气相色谱 － 质谱联用分析表明，所得木质素氢解产物(HPL)多为短链酚类化合物及含 酚羟基的芳香化合物． 将所得 HPL 代替苯酚制备糠醛 － 苯酚树脂，探究了 HPL 对苯酚的 替代率对酚醛树脂粘结强度、固含量、固化时间、游离醛含量、游离酚含量及黏度的影响． 结果表明，HPL 对苯酚的替代率为 60%时，所得酚醛树脂的粘结强度可达 2． 06MPa，游离 酚含量低于国家标准，固化时间显著缩短． 差示扫描量热分析表明，此替代率下所制备的 木质素基酚醛树脂热稳定性更好．

A hydrogenolysis process was performed for regenerated bamboo lignin after ［AMIM］OAc pretreatment by using a high-pressure batch autoclave with a rotation rate of 450r/min in 2MPa H 2 atmosphere at 260℃ for 80min,and a GC-MS analysis was conducted,finding that most hydrogenolysis products of lignin (HPL) are phenolic com- pounds with short chains or aromatic compounds containing phenol hydroxyl.Then,HPL was used as a substitution for phenol to synthesize phenol-furfural resins (PFU),and the effects of substitution rate of HPL for phenol on the bond strength,solid content,curing time,free formaldehyde content,free phenol content and viscosity of PFU were investigated.The results show that，at a substitution rate of 60%,the lignin-based PFU is of a bond strength up to 2. 06MPa as well as a free phenol content lower than those regulated by Chinese national standards,and the curing time greatly shortens.Moreover,DSC results indicate that the lignin-based PFU possesses strong thermosta- bility.